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Sol-gel modified Pechini method for obtaining

In 1967, Pechini [15] developed a process for the preparation of the precur- sor polymeric resin. First, a mixture of ions is formed in an organiccomplexingagent,CA, (citric acid or ethylenedi- aminetetraacetic acid, EDTA) and ethylene glycol solution. Second,theionsbecomeachelateandthepolymericresin forms.

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Pechini Method | Scientific.Net

Abstract: The aim of this work was to synthesize lead zirconate titanate, Pb(Zr 0.52 Ti 0.48)O 3 (PZT) via Pechini method, to characterize the polymeric precursor through differential thermal analysis and thermogravimetric analysis, as well as to characterize the PZT powder through x-ray diffraction and scanning electron microscopy with energy-dispersive spectroscopy. In this work, the metallic …

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